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Carboxymethyl Cellulose (CMC)
Methyl Cellulose (MHEC/MHPC)
Hydroxypropylmethyl Cellulose (HPMC)
Nitrocellulose (NC)
Product Range
Nitrogen Content
Viscosity
Phlegmatizers / Stabilizers
Nitrocellulose in Solution
Production
Methods of Analysis
Viscosity measurement by the Cochius method
Viscosity measurement by the ISO 14446 method
Determination of nitrogen by Schlösing-Schulze-Tiemann
Determination of the deflagration temperature
Bergmann - Junk Test
K value according to Fikentscher
Storage and Handling
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Products > Nitrocellulose (NC) > Methods of Analysis
Determination of the nitrogen content by the Schlösing-Schulze-Tiemann method
To determine the nitrogen content by the Schlösing-Schulze-Tiemann method, a precision-weighed amount of nitrocellulose is heated in the presence of iron(II) chloride and hydrochloric acid. Under these conditions nitrate is reduced to NO, which can be measured volumetrically and is proportional to the nitrogen content of the nitrocellulose. Comparison tests applying automated methods for determining the nitrogen content have repeatedly showed that the Schlösing-Schulze-Tiemann method was the most reproducible method, showing the least variations of individual readings from the mean value.

Last modified: Friday, 19.November 2004
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last modified: Friday, 19.November 2004